NurdRage
NurdRage
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  • Просмотров 113 605 975
Lab notes - Making Oleum - 20% yield improvement - (May 4th - 2024)
More lab notes on making sulfur trioxide and oleum. This time i was able to get up to 20%-25% yield with improved heating with better insulation. Also found out that precise temperature control is important and that the polymerization of the sulfur trioxide phases can be easily initiated by smearing it with a pipette on air.
Previous videos:
Purification of Sulfuric Acid by Distillation Revisited: ruclips.net/video/0Gb9rM9BJ8I/видео.html
Lab notes - Making Oleum - Success (part 1): ruclips.net/video/wB2zzm8VP9Y/видео.html
Lab notes - Making Oleum - 20% yield improvement: This Video
Donate to NurdRage!
Through Patreon (preferred): www.patreon.com/NurdRage
Through RUclips Memberships: ruclips.net/...
Просмотров: 18 565

Видео

Lab Notes - Making Oleum - Successful - (April 21-2024)
Просмотров 34 тыс.21 день назад
These are my lab notes trying to make Oleum or Fuming Sulfuric Acid by amateur means. Turns out it is possible to do it with just a ceramic hotplate, sulfuric acid, and sodium bisulfate. Along with standard laboratory glassware. But so far the yield is around 13%. I'm trying to optimize it. The procedure is simply heat the sodium bisulfate on the ceramic hotplate and pyrolyze it until it become...
Purification of Sulfuric Acid by Distillation - Revisited
Просмотров 47 тыс.Месяц назад
In this video we purify sulfuric acid again using distillation but improve our technique using a ceramic hotplate stirrer and PTFE tape to seal the joints. I start by highlighting the inherent dangers associated with handling sulfuric acid and stress the importance of safety precautions, including wearing protective clothing and performing the procedure in a well-ventilated area or fume hood. I...
Do your own Gamma Spectroscopy with the Radiacode 103
Просмотров 25 тыс.2 месяца назад
Buy the RadiaCode here: 102.radiacode.com/NurdRage In this video we review the radiacode 103, a handheld gamma ray spectrometer. We also as explore basic aspects of gamma ray spectroscopy. Geiger counters measure radiation, and they're easy to buy online. But all they do is measure how much radiation there is. The Radiacode is a gamma spectrometer and can measure the energy of each individual g...
Thanks for 2023, Channel Updates, Plans, and Thoughts
Просмотров 19 тыс.4 месяца назад
Thanks for watching! Donate to NurdRage! Through Patreon (preferred): www.patreon.com/NurdRage Through RUclips Memberships: ruclips.net/channel/UCIgKGGJkt1MrNmhq3vRibYAjoin Other RUclips channels that i think are amazing: @That_Chemist @theCodyReeder @ExplosionsAndFire @nomcopterlabs @ChemicalForce @AppliedScience @Chemiolis @chemdelic @LabCoatz_Science @AdvancedTinkering @THYZOID @NileRed Twit...
Promethean Matches - The Ancestor to Modern Matches
Просмотров 66 тыс.4 месяца назад
In this video we make the ancestor to modern matches before phosphorus: The Promethean Match The operating principle is that sulfuric acid would react with potassium chlorate and sugar to catch fire. So to turn it into a match, the sulfuric acid was stored in a glass capsule that was broken and mixed with potassium chlorate and sugar. This would ignite and set fire to the paper roll it was pack...
Make Isopropyl Nitrite without Sodium Nitrite
Просмотров 23 тыс.5 месяцев назад
In this video, we make isopropyl nitrite without using sodium nitrite. Typically, amateur chemists use sodium nitrite, hydrochloric acid, and isopropyl alcohol for this process, but sodium nitrite is becoming harder to obtain. This sodium nitrite-free pathway goes through nitrosylsulfuric acid which can be made using more easily obtained fuming nitric acid and sulfur dioxide. To make fuming nit...
This Candle MAKES Oxygen and Started a Fire on a Space Station
Просмотров 153 тыс.5 месяцев назад
In this video we make an Oxygen Candle that actually MAKES oxygen as it burns. It's also called a chemical oxygen generator. To make it, 60g of potassium chlorate are mixed with 30g of iron metal powder and 2g of calcium oxide. The powders are thoroughly mixed and initiated by direct flames or a sparkler. The reaction burns the iron powder and generates enough heat to decompose the remaining po...
How to Make Your Own Flameless Ration Heaters and the science of how they work.
Просмотров 55 тыс.5 месяцев назад
In this video we show how Flameless Ration Heaters and self heating food containers work. Inside of them is a water activated exothermic chemical reaction. The most common one is magnesium iron alloy and salt. When water is activated it produces magnesium hydroxide and plenty of heat. Less common mixtures include sodium hydroxide and aluminum, magnesium metal and sodium bisulfate, aluminum and ...
Lab Notes - Failure in Making Sodium Nitrite
Просмотров 20 тыс.6 месяцев назад
In this video i synthesize nitrosylsulfuric acid and isopropyl nitrite, and i tried to make sodium nitrite but i failed. My original goal was to make sodium nitrite. Sodium nitrite sets itself apart from the more common sodium nitrate by having one less oxygen atom, which makes it quite unstable under various conditions. This particular challenge intrigued me, and I thought I'd give it a try, e...
Make Potassium Permanganate
Просмотров 45 тыс.7 месяцев назад
In this video, we explore the preparation of potassium permanganate, a valuable oxidant with a striking purple color. Starting with 43g of manganese dioxide, often obtained from greensand filter media, and 25g of potassium chlorate, the chemicals are thoroughly mixed. A can made of iron is chosen as the reaction vessel due to its resistance to the highly corrosive mixture. All reagents are mixe...
Chemical Thunderstorm in a Beaker
Просмотров 24 тыс.7 месяцев назад
In this video we make a chemical thunderstorm in a beaker using manganese heptoxide. I wanted recreate the test tube thunderstorm on a larger scale, adding sound for a more immersive experience. The setup involved using a glass funnel to carefully pour sulfuric acid into ethanol and form a layer of it in the bottom. Sprinkling potassium permanganate into the mix led to the formation of manganes...
3 Ways to Make Sulfur Dioxide Gas
Просмотров 32 тыс.7 месяцев назад
3 Ways to Make Sulfur Dioxide Gas
Lab Equipment Repair: Broken Stirrer Encoder Disc in Hotplate Stirrer
Просмотров 14 тыс.7 месяцев назад
Lab Equipment Repair: Broken Stirrer Encoder Disc in Hotplate Stirrer
Lab notes - Making Potassium Permanganate
Просмотров 77 тыс.8 месяцев назад
Lab notes - Making Potassium Permanganate
Make Potassium Chlorate from Bleach
Просмотров 81 тыс.8 месяцев назад
Make Potassium Chlorate from Bleach
Find the Concentration of Hydrogen Peroxide by Titration with Potassium Permanganate
Просмотров 41 тыс.11 месяцев назад
Find the Concentration of Hydrogen Peroxide by Titration with Potassium Permanganate
Make Sodium Oxalate - Primary Standard for Analytical Chemistry
Просмотров 24 тыс.11 месяцев назад
Make Sodium Oxalate - Primary Standard for Analytical Chemistry
Lab Equipment: Rotary Evaporator or "Rotovap"
Просмотров 50 тыс.Год назад
Lab Equipment: Rotary Evaporator or "Rotovap"
How Does Aqua Regia Dissolve Gold and Platinum?
Просмотров 81 тыс.Год назад
How Does Aqua Regia Dissolve Gold and Platinum?
Make Sodium Hydroxide by Electrolysis with a Nafion Membrane Cell
Просмотров 46 тыс.Год назад
Make Sodium Hydroxide by Electrolysis with a Nafion Membrane Cell
Make a Nafion Divided Membrane Cell for Electrolysis
Просмотров 53 тыс.Год назад
Make a Nafion Divided Membrane Cell for Electrolysis
Lab Notes: Making Copper Sulfate and Electrobonding Wires
Просмотров 100 тыс.2 года назад
Lab Notes: Making Copper Sulfate and Electrobonding Wires
Chemical Resistance of Palladium
Просмотров 70 тыс.3 года назад
Chemical Resistance of Palladium
Efficiently Recover Nitric Acid and Copper Metal From Copper Nitrate Wastes
Просмотров 134 тыс.3 года назад
Efficiently Recover Nitric Acid and Copper Metal From Copper Nitrate Wastes
Nitric Acid Concentration and Purification (Azeotropic and Fuming)
Просмотров 136 тыс.3 года назад
Nitric Acid Concentration and Purification (Azeotropic and Fuming)
DANGEROUS reaction of ACID and GLOVES
Просмотров 58 тыс.3 года назад
DANGEROUS reaction of ACID and GLOVES
Make Nitric Acid by Thermal Decomposition of Copper Nitrate
Просмотров 70 тыс.3 года назад
Make Nitric Acid by Thermal Decomposition of Copper Nitrate
Lab Notes - August 31st - Nitric Acid from Calcium Nitrate and My Hotplate Failed, Again.
Просмотров 42 тыс.3 года назад
Lab Notes - August 31st - Nitric Acid from Calcium Nitrate and My Hotplate Failed, Again.
Make Nitric Acid from Sodium Bisulfate and Sodium Nitrate
Просмотров 132 тыс.3 года назад
Make Nitric Acid from Sodium Bisulfate and Sodium Nitrate

Комментарии

  • @mjj2u2
    @mjj2u2 День назад

    Are you connected to a Joule thief circuit. Maybe you could get some useful

  • @Tumelo-bp5zk
    @Tumelo-bp5zk День назад

    the is no acid in this video why??

  • @slfs7477
    @slfs7477 2 дня назад

    Who is here in 2024? I ended up using sea salt, and it did worked too.

  • @jesuscardben5140
    @jesuscardben5140 2 дня назад

    Hi,what Is the value ( In ohms)from that resistor hotplate ? .In my case ,Tha resistor not heating

  • @NkosinathiMconase
    @NkosinathiMconase 2 дня назад

    Wow Happy proposal Guys 💯🔥😍💖

  • @abdellahgogop5653
    @abdellahgogop5653 2 дня назад

    Is magnesium ribon 100% pure magnesium???

  • @mcdk72
    @mcdk72 2 дня назад

    Hi. Thanks for giving ideas. But your procedure is inadequate. You should try using a zerowater filter, us it out in it's tolerance 006ppm. Then regenerate it as you show and obtain the same endurance as when used first. My guess is that you get 25% using your method. Prove me wrong, or show a more adequate method. When cleaning resin include the total amount of time used, and amount of cleaning water. Use a full filter amount of resin and not just a fraction. Good luck.

    • @NurdRage
      @NurdRage 2 дня назад

      Just run a complexometric titration on a metal standard solution after putting it on the column and then eluting. You can get nearly quantitative recovery every time.

  • @Berulini
    @Berulini 2 дня назад

    Not a big addition to this video.. This is an excellent Russian dosimeter spectrometer, models radiacode 101/102/103/103g, completely Russian design, manufactured in Cyprus... also completely Russian software and Russian developers.....

  • @Berulini
    @Berulini 2 дня назад

    Not a big addition to this video.. This is an excellent Russian dosimeter spectrometer, models radiacode 101/102/103/103g, completely Russian design, manufactured in Cyprus... also completely Russian software and Russian developers.....

  • @DavidLovesBombing2
    @DavidLovesBombing2 3 дня назад

    I am going to bail out Dzhokhar Anzorovich Tsarnaev from ADX Florence

  • @JJ-qo9ik
    @JJ-qo9ik 3 дня назад

    can you use salt water to regenerate?

  • @yassersalah7439
    @yassersalah7439 3 дня назад

    Can we add H2O2 to decompose the organic additives and then distill the hydrogen peroxide and water at 150C? This way, we do not have to go to 350C to distill the acid itself. Please advise.

  • @jogandsp
    @jogandsp 4 дня назад

    A nurdrage short???

  • @rahultripathi5155
    @rahultripathi5155 4 дня назад

    Science is really important....:)

  • @laurenceperkins7468
    @laurenceperkins7468 4 дня назад

    Does the density of dioxane happen to be greater than the sodium, but less than the slag perchance? Sodium floating on it doesn't help much if the stuff you're separating it from floats too...

  • @Salt_and_Peroxide
    @Salt_and_Peroxide 5 дней назад

    Man I love old nurdrage

  • @ronishbarakoti4371
    @ronishbarakoti4371 5 дней назад

    Hi, Any chemical or liquid combination can make glow bright white light continues 1 month. Is it possible to make it?

  • @DrCarstairs
    @DrCarstairs 6 дней назад

    👍

  • @rtcoleman3626
    @rtcoleman3626 6 дней назад

    🇺🇸👍👍💯🇺🇸

  • @GTSongwriter
    @GTSongwriter 6 дней назад

    Is there any way to test it, to see if it's working correctly?

  • @ijheller
    @ijheller 6 дней назад

    "At least it's a cool demo on ice expansion." I see what you did there.

  • @tomoyaokazaki6021
    @tomoyaokazaki6021 6 дней назад

    What if you mixed the isopropyl nitrite with another sodium salt like chloride? Could that preform the ion swap and let the sodium nitrite precipitate out? Im also an amature chemist trying to figure this out haha

  • @tomoyaokazaki6021
    @tomoyaokazaki6021 6 дней назад

    My favorite chemistry youtuber. Also can you use this method to create sodium nitrite?

  • @kaikaki3137
    @kaikaki3137 6 дней назад

    Heya NR, I'm not a Chemist in any way what-so-ever, but I've been watching you steadily since Dec 2014! I hope never to hear your real voice, I hope never to see your face because I love the Mystery behind the man; and your fantastic humor that inject here and there. Despite not being a chemist I've learned loads from you and several other Chem-Tubers (like Chemplayer) and it's amazing how often I actually recall the knowledge when I have to inform friends/family of Chemistry facts for whatever reason(s); and all from simply watching your videos casually. Stay awesome man.

  • @user-oo3pq3hd5y
    @user-oo3pq3hd5y 7 дней назад

    That's actually not too bad!

  • @eventsigil9176
    @eventsigil9176 7 дней назад

    Instead of sodium hypochlorite, why not use calcium hypochlorite?

  • @Tim99-lg7kn
    @Tim99-lg7kn 7 дней назад

    If you gently take a latex-free eraser you can shine that coin and get rid of that pink copper look and restore more of the natural copper look. You just have to be super gentle and I don't recommend doing it to any coin that's valuable or truly collectible

  • @rhondaljhuziz9054
    @rhondaljhuziz9054 7 дней назад

    I've been watching your videos and learned me a lot,once you make a new video add some funny impression, like the laugh of mad scientists,successfully creating his experiments

  • @theshuman100
    @theshuman100 7 дней назад

    now to make petr and combine the two

  • @xXZer0Lecam0nXx
    @xXZer0Lecam0nXx 7 дней назад

    Man, I missed this channel. Is it possible that running the distillation slightly slower could have a positive effect on yield? Also, could you figure out an average time @ specific temp to use as a guide of when to stop the distillation instead of opening the system?

  • @christopherleubner6633
    @christopherleubner6633 7 дней назад

    Distill our HBr and HI acids under reduced pressure and under yellow light. Make as needed and use immediatly, if you must store them for any time purge the bottle with nitrogen or argon and in a fridge. ❤

  • @lanehaden3457
    @lanehaden3457 8 дней назад

    ni neccesary

  • @JehuMcSpooran
    @JehuMcSpooran 8 дней назад

    Ok, who else wants to see the "spicy flesh eating wax" vs a chicken leg?

  • @GameDesignerJDG
    @GameDesignerJDG 8 дней назад

    My dad works with SO3 sometimes. Rough, but can be done safely.

  • @user-el4np5xt8c
    @user-el4np5xt8c 9 дней назад

    Here for Ze Mandatory Comment

  • @dustinbarks435
    @dustinbarks435 9 дней назад

    Could u use calcium hypochlorite from say pool shock and potassium chloride in a cell like this ?

  • @aizathays4429
    @aizathays4429 9 дней назад

    hi Could you make potassium perchlorate?

  • @letmepicyou
    @letmepicyou 9 дней назад

    Greetings from Ohio! I had a non-related (to Oleum) question for you - have you ever tried using a "hydrogen water generator bottle" as a chlorate cell? I got my hands on one, and was sitting there pondering my supply of potassium chloride and thought my "hydrogen water generator" might better serve me as a chlorate cell...any thoughts?

  • @bigonprivacy2708
    @bigonprivacy2708 9 дней назад

    This little video of predictive programming brought to you by The World Economici Forum, Pfizer, and the ADL.

  • @benwelborn8828
    @benwelborn8828 9 дней назад

    A wayward thought... aerosolized hydrogen peroxide is suspected to cause SO3 formation in the environment. I'm not sure what method would be best for aerosolizing H2O2, but there are peroxide fogging machines for sale (not sure how they're different from water foggers); I wonder whether one of those cheap atomization discs might work. Also, the logistics of combining gases might be an issue. In my experience, the vapor from those atomizers tend to be cold and fall, so perhaps just introducing concentrated peroxide vapor from somewhere above the distilling flask would help, especially at the later stage, when more water begins to form in the distilling flask, anyway.

    • @benwelborn8828
      @benwelborn8828 9 дней назад

      A second (possibly better) wayward thought... perhaps a dessicant (another sulfate?) could be added, if moisture is the reason the reaction is stopping short.

    • @benwelborn8828
      @benwelborn8828 9 дней назад

      A third wayward thought... perhaps you could use a two necked receiving flask and a glass rod, or maybe dangle (with string made of teflon tape) a seeding spot, near the end of the condenser, as an indicator, so that you aren't forming crystals that block the condenser.

  • @midwestchem368
    @midwestchem368 9 дней назад

    No! Not getting a job!! 😂😂😂

  • @flubalubaful
    @flubalubaful 9 дней назад

    If they could get 1 amp, from each battery at 4 volts this type of cell could be combined to make a 48v battery with 12 cells pushing out 12 amps x this by 100 and you have a very impresive power source. More than enough to charge a larger battery for however long each cell lasts, put everything in a clear packaging allowing it to absorb natural light and you have a solar panel that generates power all night and more during the day. It is just getting it up to 1 amp which means experimenting with solar panel used and size.

  • @jamesemerson7445
    @jamesemerson7445 9 дней назад

    My favorite part of the video was the sneaky diss on Nigel at the end. 😂

  • @antiisocial
    @antiisocial 9 дней назад

    Yo!!